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Titre: Structural, morphological, and magnetic properties of electrodeposited coNi thin films on the FTO substrate
Auteur(s): Boulegane, Ala
Guittoum, Abderrahim
Laggoun, Ali
Boudissa, Mokhtar
Hemmous, Messaoud
Mots-clés: CoNi thin films
FTO
Magnetic properties
Morphology
Potential
Structural properties
Date de publication: 2022
Editeur: Springer
Collection/Numéro: Journal of Superconductivity and Novel Magnetism/ Vol.35, N°9 (2022);pp. 2583-2593
Résumé: CoNi films were elaborated by electrodeposition onto FTO substrates using a chloride bath with a metallic ion molar ratio [Co2+]/[Ni2+] equals 1/1. Three samples were elaborated for different potentials ranging from −1.6 to −1.5 V. The structure and the morphology of CoNi films were studied using X-ray diffraction (XRD), scanning electron microscopy (SEM), and atomic force microscopy (AFM). The chemical compositions are obtained using energy dispersive X-ray (EDX) and the magnetic properties were studied using a vibrating sample magnetometer (VSM). From X-ray diffraction, we have shown the presence of the FCC phase of CoNi binary alloy with a well-pronounced texture along the < 111 > , < 200 > , and < 220 > planes for all samples. We have found that the applied potential has an influence on crystallite sizes. Besides, a moderate change in the lattice parameter has been observed with increasing applied potential. The AFM images show that the applied potential changes the morphology and the surface roughness of CoNi films. In addition, the SEM images confirm the granular morphology of CoNi deposits and show a good relationship between voltage and grain size. The EDX spectrums confirm the deposition of the cobalt and the nickel on the FTO substrate and show the precedence deposition of Co compared with Ni. The extracted coercive field Hc and squareness from the hysteresis loops explained the good correlation between the magnetic and structural properties of CoNi thin films
URI/URL: DOI 10.1007/s10948-022-06308-3
https://link.springer.com/article/10.1007/s10948-022-06308-3
http://dlibrary.univ-boumerdes.dz:8080/handle/123456789/10225
ISSN: 15571939
Collection(s) :Publications Internationales

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